Aluminium surface modification by nitrogen-argon mixture PIII
Pure nitrogen, 30% argon/70% nitrogen, 50% argon/50% nitrogen, 70% argon/30% nitrogen plasma immersion ion implantation (PIII) processes onto aluminium samples has been performed at 2 to 6 kV negative bias and 50 to 150 us pulse widths, the sample temperature being established at 400 °C. Incident fluencies of ~10(18) atoms/cm² were used to investigate the diffusion behaviour and AlN phase formation in the samples. X-ray diffraction (XRD) shows the formation of the cubic phase of AlN with both pure nitrogen and all the mixtures whereas the hexagonal phase becomes apparent only in the 50% mixture and in pure nitrogen. The characteristic peak of AlN has also been determined by Raman spectroscopy. The microhardness was found to be always maximal with the 50% nitrogen 50% argon mixture.
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Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C.
2009
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oai:scielo:S1665-352120090002000032013-11-28Aluminium surface modification by nitrogen-argon mixture PIIIMillán-Flores,H.López-Callejas,R.Granda-Gutiérrez,E. E.de la Piedad-Benítez,A.Muñóz-Castro,A. E.Valencia A.,R.Peña-Eguiluz,R.Mercado-Cabrera,A.Barocio,S. R. plasma immersion ion implantation X-ray diffraction hardness scanning electron microscopy surface modification Pure nitrogen, 30% argon/70% nitrogen, 50% argon/50% nitrogen, 70% argon/30% nitrogen plasma immersion ion implantation (PIII) processes onto aluminium samples has been performed at 2 to 6 kV negative bias and 50 to 150 us pulse widths, the sample temperature being established at 400 °C. Incident fluencies of ~10(18) atoms/cm² were used to investigate the diffusion behaviour and AlN phase formation in the samples. X-ray diffraction (XRD) shows the formation of the cubic phase of AlN with both pure nitrogen and all the mixtures whereas the hexagonal phase becomes apparent only in the 50% mixture and in pure nitrogen. The characteristic peak of AlN has also been determined by Raman spectroscopy. The microhardness was found to be always maximal with the 50% nitrogen 50% argon mixture.info:eu-repo/semantics/openAccessSociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C.Superficies y vacío v.22 n.2 20092009-06-01info:eu-repo/semantics/articletext/htmlhttp://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S1665-35212009000200003en |
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author |
Millán-Flores,H. López-Callejas,R. Granda-Gutiérrez,E. E. de la Piedad-Benítez,A. Muñóz-Castro,A. E. Valencia A.,R. Peña-Eguiluz,R. Mercado-Cabrera,A. Barocio,S. R. |
spellingShingle |
Millán-Flores,H. López-Callejas,R. Granda-Gutiérrez,E. E. de la Piedad-Benítez,A. Muñóz-Castro,A. E. Valencia A.,R. Peña-Eguiluz,R. Mercado-Cabrera,A. Barocio,S. R. Aluminium surface modification by nitrogen-argon mixture PIII |
author_facet |
Millán-Flores,H. López-Callejas,R. Granda-Gutiérrez,E. E. de la Piedad-Benítez,A. Muñóz-Castro,A. E. Valencia A.,R. Peña-Eguiluz,R. Mercado-Cabrera,A. Barocio,S. R. |
author_sort |
Millán-Flores,H. |
title |
Aluminium surface modification by nitrogen-argon mixture PIII |
title_short |
Aluminium surface modification by nitrogen-argon mixture PIII |
title_full |
Aluminium surface modification by nitrogen-argon mixture PIII |
title_fullStr |
Aluminium surface modification by nitrogen-argon mixture PIII |
title_full_unstemmed |
Aluminium surface modification by nitrogen-argon mixture PIII |
title_sort |
aluminium surface modification by nitrogen-argon mixture piii |
description |
Pure nitrogen, 30% argon/70% nitrogen, 50% argon/50% nitrogen, 70% argon/30% nitrogen plasma immersion ion implantation (PIII) processes onto aluminium samples has been performed at 2 to 6 kV negative bias and 50 to 150 us pulse widths, the sample temperature being established at 400 °C. Incident fluencies of ~10(18) atoms/cm² were used to investigate the diffusion behaviour and AlN phase formation in the samples. X-ray diffraction (XRD) shows the formation of the cubic phase of AlN with both pure nitrogen and all the mixtures whereas the hexagonal phase becomes apparent only in the 50% mixture and in pure nitrogen. The characteristic peak of AlN has also been determined by Raman spectroscopy. The microhardness was found to be always maximal with the 50% nitrogen 50% argon mixture. |
publisher |
Sociedad Mexicana de Ciencia y Tecnología de Superficies y Materiales A.C. |
publishDate |
2009 |
url |
http://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S1665-35212009000200003 |
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