Chromatographic Methods [electronic resource] /

1 Introduction -- 1.1 Introduction to chromatography -- 1.2 History of chromatography -- 1.3 Classification of chromatographic methods -- References -- 2 Theoretical considerations -- 2.1 Introduction -- 2.2 Factors influencing retention -- 2.3 Retention and equilibrium in chromatography -- 2.4 Separating efficiency of a column -- 2.5 Band broadening processes -- 2.6 Resolution -- 2.7 Quantification in chromatography -- References -- 3 Planar chromatography -- 3.1 Thin layer chromatography -- 3.2 Paper chromatography -- 3.3 Electrophoresis -- 3.4 Capillary electrophoresis -- References -- 4 Liquid phase chromatography on open columns -- 4.1 Introduction -- 4.2 Practical aspects and considerations -- 4.3 Modes of chromatography -- 4.4 Adsorption chromatography -- 4.5 Partition column chromatography -- 4.6 Ion exchange chromatography -- 4.7 Inorganic ion exchangers -- 4.8 Gel ion exchangers -- 4.9 Gel chromatography -- 4.10 Affinity chromatography -- 4.11 Covalent chromatography -- 4.12 Chromatofocusing -- 4.13 Flash chromatography -- References -- 5 Gas chromatography -- 5.1 Introduction -- 5.2 Principles of gas chromatography -- 5.3 Resolution -- 5.4 Columns and stationary phase -- 5.5 Choice of stationary phase -- 5.6 Capillary column gas chromatography -- 5.7 Gas-solid chromatography -- 5.8 Gas chromatography instrumentation -- 5.9 Sampling techniques -- 5.10 Detectors for gas chromatography -- 5.11 Supercritical gas chromatography -- 5.12 Applications of gas chromatography -- References -- 6 High performance liquid chromatography -- 6.1 Introduction -- 6.2 Modes of chromatography -- 6.3 Overview of high performance liquid chromatography instrumentation -- 6.4 Theory -- 6.5 Detailed discussion of high performance liquid chromatography instrumentation -- 6.6 Column packings and stationary phases for liquid chromatography -- 6.7 Adsorption chromatography -- 6.8 Liquid—liquid partition chromatography -- 6.9 Chemically bonded stationary phases for high performance liquid chromatography -- 6.10 Chiral chromatography -- 6.11 Ion exchange chromatography -- 6.12 Ion pairing -- 6.13 Size exclusion chromatography -- 6.14 Liquid chromatography method development -- 6.15 Quantitative analysis -- 6.16 Preparative liquid chromatography -- 6.17 Microcolumns in liquid chromatography -- 6.18 Applications -- References -- 7 Chromatography and spectroscopic techniques -- 7.1 Introduction -- 7.2 Chromatographic requirements -- 7.3 Chromatographic and mass spectrometry techniques -- 7.4 Gas chromatography interfacing techniques -- 7.5 High performance liquid chromatography interfacing -- 7.6 Chromatography and mass spectrometry data systems -- 7.7 Infrared spectrophotometry -- 7.8 Ultraviolet—visible spectrophotometry -- 7.9 Atomic spectroscopy -- References -- 8 Processing chromatographic data -- 8.1 Introduction -- 8.2 The chromatogram -- 8.3 Data collection and processing -- 8.4 Chromatography software -- 8.5 Method development and optimisation -- 8.6 Laboratory information management systems -- References -- 9 Model or practical experiments in chromatographic techniques -- 9.1 Introduction -- 9.2 List of experiments -- 9.3 Section A. Paper chromatography -- 9.4 Section B. Electrophoresis and related techniques -- 9.5 Section C. Thin layer chromatography -- 9.6 Section D. Column chromatography -- 9.7 Section E. Gas chromatography -- 9.8 Section F. High performance liquid chromatography -- 9.9 Section G. Capillary electrophoresis -- References -- 10 Illustrative problems in chromatography -- 10.1 Introduction -- 10.2 Plate theory and resolution -- 10.3 Van Deemter -- 10.4 Volatility and temperature in gas chromatography -- 10.5 Qualitative analysis -- 10.6 Quantitative analysis -- 10.7 Composite questions -- Appendix 1 Glossary of chromatographic terms -- Appendix 2 Table of chromatography symbols.

Bibliographic Details

Main Authors:	Braithwaite, A. author., Smith, F. J. author., SpringerLink (Online service)
Format:	Texto biblioteca
Language:	eng
Published:	Dordrecht : Springer Netherlands : Imprint: Springer, 1999
Subjects:	Chemistry., Analytical chemistry., Physical chemistry., Analytical Chemistry., Physical Chemistry.,
Online Access:	http://dx.doi.org/10.1007/978-94-011-0599-6
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