Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size

Abstract The use of biodegradable polymers to encapsulate fertilizers is one of the main tools that help to prevent them to get carried away by the irrigation water, since phosphate based fertilizers are highly soluble. Indeed, this technology might improve productivity and reduce both costs and environmental pollution. In this work potassium phosphate was encapsulated in chitosan, which is one of the most abundant natural and biodegradable polymers widely applied in agriculture for plant defense and yield increase, applying the encapsulation method of spray drying to provide a high encapsulation efficiency rates. A 2k factorial design was implemented to evaluate the effect of the different operational parameters of the spray dryer on the particle size, measured by scan electronic microscopy, then it was obtained the average particle sizes to be between 1.08 to 2.04 µm. The release of KH2PO4 from chitosan spheres of different sizes was performed in Milli-Q water and was measured using the conductometry technique. The experiments revealed that the parameter with the greatest effect was the feed rate, and that the system with the smallest particle size obtained (1.08 µm) showed a slower release without losing an important amount of encapsulation efficiency.

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Main Authors: Colorado Olivares,Enrique, Olivares-Romero,José Luis, Barrera-Méndez,Felipe
Format: Digital revista
Language:English
Published: Sociedad Química de México A.C. 2018
Online Access:http://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S1870-249X2018000300067
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spelling oai:scielo:S1870-249X20180003000672020-07-01Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle SizeColorado Olivares,EnriqueOlivares-Romero,José LuisBarrera-Méndez,Felipe Microencapsulation Chitosan Fertilizer Phosphate Spray Dryer Abstract The use of biodegradable polymers to encapsulate fertilizers is one of the main tools that help to prevent them to get carried away by the irrigation water, since phosphate based fertilizers are highly soluble. Indeed, this technology might improve productivity and reduce both costs and environmental pollution. In this work potassium phosphate was encapsulated in chitosan, which is one of the most abundant natural and biodegradable polymers widely applied in agriculture for plant defense and yield increase, applying the encapsulation method of spray drying to provide a high encapsulation efficiency rates. A 2k factorial design was implemented to evaluate the effect of the different operational parameters of the spray dryer on the particle size, measured by scan electronic microscopy, then it was obtained the average particle sizes to be between 1.08 to 2.04 µm. The release of KH2PO4 from chitosan spheres of different sizes was performed in Milli-Q water and was measured using the conductometry technique. The experiments revealed that the parameter with the greatest effect was the feed rate, and that the system with the smallest particle size obtained (1.08 µm) showed a slower release without losing an important amount of encapsulation efficiency.info:eu-repo/semantics/openAccessSociedad Química de México A.C.Journal of the Mexican Chemical Society v.62 n.3 20182018-09-01info:eu-repo/semantics/articletext/htmlhttp://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S1870-249X2018000300067en10.29356/jmcs.v62i3.452
institution SCIELO
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country México
countrycode MX
component Revista
access En linea
databasecode rev-scielo-mx
tag revista
region America del Norte
libraryname SciELO
language English
format Digital
author Colorado Olivares,Enrique
Olivares-Romero,José Luis
Barrera-Méndez,Felipe
spellingShingle Colorado Olivares,Enrique
Olivares-Romero,José Luis
Barrera-Méndez,Felipe
Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size
author_facet Colorado Olivares,Enrique
Olivares-Romero,José Luis
Barrera-Méndez,Felipe
author_sort Colorado Olivares,Enrique
title Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size
title_short Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size
title_full Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size
title_fullStr Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size
title_full_unstemmed Microencapsulation of Potassium Phosphate in Chitosan and the Effect of Spray Drying Operating Variables on the Particle Size
title_sort microencapsulation of potassium phosphate in chitosan and the effect of spray drying operating variables on the particle size
description Abstract The use of biodegradable polymers to encapsulate fertilizers is one of the main tools that help to prevent them to get carried away by the irrigation water, since phosphate based fertilizers are highly soluble. Indeed, this technology might improve productivity and reduce both costs and environmental pollution. In this work potassium phosphate was encapsulated in chitosan, which is one of the most abundant natural and biodegradable polymers widely applied in agriculture for plant defense and yield increase, applying the encapsulation method of spray drying to provide a high encapsulation efficiency rates. A 2k factorial design was implemented to evaluate the effect of the different operational parameters of the spray dryer on the particle size, measured by scan electronic microscopy, then it was obtained the average particle sizes to be between 1.08 to 2.04 µm. The release of KH2PO4 from chitosan spheres of different sizes was performed in Milli-Q water and was measured using the conductometry technique. The experiments revealed that the parameter with the greatest effect was the feed rate, and that the system with the smallest particle size obtained (1.08 µm) showed a slower release without losing an important amount of encapsulation efficiency.
publisher Sociedad Química de México A.C.
publishDate 2018
url http://www.scielo.org.mx/scielo.php?script=sci_arttext&pid=S1870-249X2018000300067
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