Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel

ABSTRACT In this work the reversion of the strain-induced ?’-martensite to ?’-austenite was studied in a series of AISI 316 stainless steels (SS) specimens. The samples were submitted to 63% reduction in thickness by rolling at a temperature of -70ºC, to achieve high martensite content. The reversion of martensite to austenite was made by means of isochronic, isothermal heat treatments at temperatures between 200 and 900ºC, so as to induce partial martensite-austenite phase transformation. The samples were studied by optical and electronic microscopy, X-ray diffraction, magnetization measurements, microhardness, and electromagnetic non destructive methods: feritscope, conductivity measurements using Van der Pauw’s technique, and magnetic permeability assessments by an eddy current inverse method. The metalography study showed an ?’ lath martensite type structure and a similar one for the reverted austenite (?’). Magnetization measurements and magnetic permeability showed that the reversion is active between 400 and 800°C. From the magnetic saturation measurements, a new calibration curve for the assessment of %?’ through the feritscope readings was obtained. The results of the different techniques were com-pared, in order to assess the scope of the studied techniques in the characterization of rolled SS products, and in the evaluation of progress of reversion reaction.

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Main Authors: Fava,Javier, Spinosa,Cristina, Ruch,Marta, Carabedo,Fernando, Landau,Mónica, Cosarinsky,Guillermo, Savin,Adriana, Steigmann,Rozina, Craus,Mihail Liviu
Format: Digital revista
Language:English
Published: Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro 2018
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523
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spelling oai:scielo:S1517-707620180002005232018-07-19Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steelFava,JavierSpinosa,CristinaRuch,MartaCarabedo,FernandoLandau,MónicaCosarinsky,GuillermoSavin,AdrianaSteigmann,RozinaCraus,Mihail Liviu Martensite reversion austenitic eddy current. ABSTRACT In this work the reversion of the strain-induced ?’-martensite to ?’-austenite was studied in a series of AISI 316 stainless steels (SS) specimens. The samples were submitted to 63% reduction in thickness by rolling at a temperature of -70ºC, to achieve high martensite content. The reversion of martensite to austenite was made by means of isochronic, isothermal heat treatments at temperatures between 200 and 900ºC, so as to induce partial martensite-austenite phase transformation. The samples were studied by optical and electronic microscopy, X-ray diffraction, magnetization measurements, microhardness, and electromagnetic non destructive methods: feritscope, conductivity measurements using Van der Pauw’s technique, and magnetic permeability assessments by an eddy current inverse method. The metalography study showed an ?’ lath martensite type structure and a similar one for the reverted austenite (?’). Magnetization measurements and magnetic permeability showed that the reversion is active between 400 and 800°C. From the magnetic saturation measurements, a new calibration curve for the assessment of %?’ through the feritscope readings was obtained. The results of the different techniques were com-pared, in order to assess the scope of the studied techniques in the characterization of rolled SS products, and in the evaluation of progress of reversion reaction.info:eu-repo/semantics/openAccessLaboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiroem cooperação com a Associação Brasileira do Hidrogênio, ABH2Matéria (Rio de Janeiro) v.23 n.2 20182018-01-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523en10.1590/s1517-707620180002.04
institution SCIELO
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libraryname SciELO
language English
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author Fava,Javier
Spinosa,Cristina
Ruch,Marta
Carabedo,Fernando
Landau,Mónica
Cosarinsky,Guillermo
Savin,Adriana
Steigmann,Rozina
Craus,Mihail Liviu
spellingShingle Fava,Javier
Spinosa,Cristina
Ruch,Marta
Carabedo,Fernando
Landau,Mónica
Cosarinsky,Guillermo
Savin,Adriana
Steigmann,Rozina
Craus,Mihail Liviu
Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
author_facet Fava,Javier
Spinosa,Cristina
Ruch,Marta
Carabedo,Fernando
Landau,Mónica
Cosarinsky,Guillermo
Savin,Adriana
Steigmann,Rozina
Craus,Mihail Liviu
author_sort Fava,Javier
title Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_short Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_full Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_fullStr Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_full_unstemmed Characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
title_sort characterization of reverse martensitic transformation in cold-rolled austenitic 316 stainless steel
description ABSTRACT In this work the reversion of the strain-induced ?’-martensite to ?’-austenite was studied in a series of AISI 316 stainless steels (SS) specimens. The samples were submitted to 63% reduction in thickness by rolling at a temperature of -70ºC, to achieve high martensite content. The reversion of martensite to austenite was made by means of isochronic, isothermal heat treatments at temperatures between 200 and 900ºC, so as to induce partial martensite-austenite phase transformation. The samples were studied by optical and electronic microscopy, X-ray diffraction, magnetization measurements, microhardness, and electromagnetic non destructive methods: feritscope, conductivity measurements using Van der Pauw’s technique, and magnetic permeability assessments by an eddy current inverse method. The metalography study showed an ?’ lath martensite type structure and a similar one for the reverted austenite (?’). Magnetization measurements and magnetic permeability showed that the reversion is active between 400 and 800°C. From the magnetic saturation measurements, a new calibration curve for the assessment of %?’ through the feritscope readings was obtained. The results of the different techniques were com-pared, in order to assess the scope of the studied techniques in the characterization of rolled SS products, and in the evaluation of progress of reversion reaction.
publisher Laboratório de Hidrogênio, Coppe - Universidade Federal do Rio de Janeiro
publishDate 2018
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S1517-70762018000200523
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