![CRYSTAL STRUCTURE OF 5,6,812b-TETRAHYDRODIOXOLO]4,5-g]ISOINDOLO[1,2-a]ISOQUINOLIN-8-ONE (C17H13NO3)](/search/themes/bootstrap3/images/revista.png)
CRYSTAL STRUCTURE OF 5,6,812b-TETRAHYDRODIOXOLO]4,5-g]ISOINDOLO[1,2-a]ISOQUINOLIN-8-ONE (C17H13NO3)
The title compound was prepared by cyclization of 2-(3,4-methylenedioxyphenyl)ethyl-3-hydroxyisoindolin-l-one in concentrated hydrochloric acid. The compound crystallizes in the orthorhombic space group Pca2(1) (No. 29) with a = 27.034(5) Å, b = 4.5093(9) Å, c = 10.667(2)Å, V = 1300.4(4) ų and Z = 4. The crystal consists of a single enantiomer. The molecule consists of two essentially flat moieties forming an dihedral angle of 116.3(2)°. The crystal slructure has intermolecular C-H-O interactions resulting in chains that run along the crystallographic c-axis.
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| Main Authors: | , , |
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| Format: | Digital revista |
| Language: | English |
| Published: |
Sociedad Chilena de Química
2009
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| Online Access: | http://www.scielo.cl/scielo.php?script=sci_arttext&pid=S0717-97072009000300026 |
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