SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION

ABSTRACT Extracts from the leaves of Psidium guajava L have been studied due to their importance as a source of natural antioxidant components with possible applications in the pharmaceutical and food industries. In this work, the sequential use of steam distillation and supercritical fluid extraction was studied to obtain the essential oil from the leaves and non-volatile compounds from the residue. The non-volatile compounds were obtained by CO2 supercritical extraction. Experiments were performed in a automated pilot-scale extractor at constant pressure of 15 MPa, at 313 K and 333 K in three different flow rate conditions. The analysis of the essential oil with GC-MS identified E-caryophyllene, β-selinene1, α-selinene, selin-11-en-4-α-ol and E-nerolidol as main compounds. Antioxidant activity was observed in all extracts. The experimental extraction curves were compared to simulated ones predicted by a mathematical model based on mass transfer principles with two adjustable parameters. The model used fitted accurately the experimental data.

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Main Authors: Silva,Caroline G. F. da, Lucas,Aline M., Santo,Alexandre T. do E., Almeida,Rafael N., Cassel,Eduardo, Vargas,Rubem M. F.
Format: Digital revista
Language:English
Published: Brazilian Society of Chemical Engineering 2019
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322019000100487
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spelling oai:scielo:S0104-663220190001004872019-07-10SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTIONSilva,Caroline G. F. daLucas,Aline M.Santo,Alexandre T. do E.Almeida,Rafael N.Cassel,EduardoVargas,Rubem M. F. Supercritical fluid extraction Psidium guajava L. Essential oil Antioxidant compounds ABSTRACT Extracts from the leaves of Psidium guajava L have been studied due to their importance as a source of natural antioxidant components with possible applications in the pharmaceutical and food industries. In this work, the sequential use of steam distillation and supercritical fluid extraction was studied to obtain the essential oil from the leaves and non-volatile compounds from the residue. The non-volatile compounds were obtained by CO2 supercritical extraction. Experiments were performed in a automated pilot-scale extractor at constant pressure of 15 MPa, at 313 K and 333 K in three different flow rate conditions. The analysis of the essential oil with GC-MS identified E-caryophyllene, β-selinene1, α-selinene, selin-11-en-4-α-ol and E-nerolidol as main compounds. Antioxidant activity was observed in all extracts. The experimental extraction curves were compared to simulated ones predicted by a mathematical model based on mass transfer principles with two adjustable parameters. The model used fitted accurately the experimental data.info:eu-repo/semantics/openAccessBrazilian Society of Chemical EngineeringBrazilian Journal of Chemical Engineering v.36 n.1 20192019-03-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322019000100487en10.1590/0104-6632.20190361s20170215
institution SCIELO
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country Brasil
countrycode BR
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databasecode rev-scielo-br
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region America del Sur
libraryname SciELO
language English
format Digital
author Silva,Caroline G. F. da
Lucas,Aline M.
Santo,Alexandre T. do E.
Almeida,Rafael N.
Cassel,Eduardo
Vargas,Rubem M. F.
spellingShingle Silva,Caroline G. F. da
Lucas,Aline M.
Santo,Alexandre T. do E.
Almeida,Rafael N.
Cassel,Eduardo
Vargas,Rubem M. F.
SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION
author_facet Silva,Caroline G. F. da
Lucas,Aline M.
Santo,Alexandre T. do E.
Almeida,Rafael N.
Cassel,Eduardo
Vargas,Rubem M. F.
author_sort Silva,Caroline G. F. da
title SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION
title_short SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION
title_full SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION
title_fullStr SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION
title_full_unstemmed SEQUENTIAL PROCESSING OF Psidium guajava L. LEAVES: STEAM DISTILLATION AND SUPERCRITICAL FLUID EXTRACTION
title_sort sequential processing of psidium guajava l. leaves: steam distillation and supercritical fluid extraction
description ABSTRACT Extracts from the leaves of Psidium guajava L have been studied due to their importance as a source of natural antioxidant components with possible applications in the pharmaceutical and food industries. In this work, the sequential use of steam distillation and supercritical fluid extraction was studied to obtain the essential oil from the leaves and non-volatile compounds from the residue. The non-volatile compounds were obtained by CO2 supercritical extraction. Experiments were performed in a automated pilot-scale extractor at constant pressure of 15 MPa, at 313 K and 333 K in three different flow rate conditions. The analysis of the essential oil with GC-MS identified E-caryophyllene, β-selinene1, α-selinene, selin-11-en-4-α-ol and E-nerolidol as main compounds. Antioxidant activity was observed in all extracts. The experimental extraction curves were compared to simulated ones predicted by a mathematical model based on mass transfer principles with two adjustable parameters. The model used fitted accurately the experimental data.
publisher Brazilian Society of Chemical Engineering
publishDate 2019
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322019000100487
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