Experimental study of a rotating packed bed distillation column

The purpose of this work was to study the mass transfer performance of rotating packed beds applying the "Higee" process. The operations were carried out with the n-hexane/n-heptane distilling system at atmospheric pressure and under total reflux conditions. The rotating speed could be varied between 300 and 2500 rpm, which provided centrifugal forces from 5 to 316 times the Earth's gravity. The effects of concentration, vapor velocity, rotating speed and packing type (two different Raschig ring sizes and structured wire mesh packing) on mass transfer behavior were analyzed. Experimental results showed that the mass transfer coefficient depends on the liquid flow rates and rotating speed. The equipment had high separation efficiency in a reduced bed volume.

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Bibliographic Details
Main Authors: Nascimento,J. V. S., Ravagnani,T. M. K., Pereira,J. A. F. R.
Format: Digital revista
Language:English
Published: Brazilian Society of Chemical Engineering 2009
Online Access:http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322009000100021
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spelling oai:scielo:S0104-663220090001000212009-03-10Experimental study of a rotating packed bed distillation columnNascimento,J. V. S.Ravagnani,T. M. K.Pereira,J. A. F. R. Distillation Mass transfer coefficient Rotating packed bed The purpose of this work was to study the mass transfer performance of rotating packed beds applying the "Higee" process. The operations were carried out with the n-hexane/n-heptane distilling system at atmospheric pressure and under total reflux conditions. The rotating speed could be varied between 300 and 2500 rpm, which provided centrifugal forces from 5 to 316 times the Earth's gravity. The effects of concentration, vapor velocity, rotating speed and packing type (two different Raschig ring sizes and structured wire mesh packing) on mass transfer behavior were analyzed. Experimental results showed that the mass transfer coefficient depends on the liquid flow rates and rotating speed. The equipment had high separation efficiency in a reduced bed volume.info:eu-repo/semantics/openAccessBrazilian Society of Chemical EngineeringBrazilian Journal of Chemical Engineering v.26 n.1 20092009-03-01info:eu-repo/semantics/articletext/htmlhttp://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322009000100021en10.1590/S0104-66322009000100021
institution SCIELO
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country Brasil
countrycode BR
component Revista
access En linea
databasecode rev-scielo-br
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region America del Sur
libraryname SciELO
language English
format Digital
author Nascimento,J. V. S.
Ravagnani,T. M. K.
Pereira,J. A. F. R.
spellingShingle Nascimento,J. V. S.
Ravagnani,T. M. K.
Pereira,J. A. F. R.
Experimental study of a rotating packed bed distillation column
author_facet Nascimento,J. V. S.
Ravagnani,T. M. K.
Pereira,J. A. F. R.
author_sort Nascimento,J. V. S.
title Experimental study of a rotating packed bed distillation column
title_short Experimental study of a rotating packed bed distillation column
title_full Experimental study of a rotating packed bed distillation column
title_fullStr Experimental study of a rotating packed bed distillation column
title_full_unstemmed Experimental study of a rotating packed bed distillation column
title_sort experimental study of a rotating packed bed distillation column
description The purpose of this work was to study the mass transfer performance of rotating packed beds applying the "Higee" process. The operations were carried out with the n-hexane/n-heptane distilling system at atmospheric pressure and under total reflux conditions. The rotating speed could be varied between 300 and 2500 rpm, which provided centrifugal forces from 5 to 316 times the Earth's gravity. The effects of concentration, vapor velocity, rotating speed and packing type (two different Raschig ring sizes and structured wire mesh packing) on mass transfer behavior were analyzed. Experimental results showed that the mass transfer coefficient depends on the liquid flow rates and rotating speed. The equipment had high separation efficiency in a reduced bed volume.
publisher Brazilian Society of Chemical Engineering
publishDate 2009
url http://old.scielo.br/scielo.php?script=sci_arttext&pid=S0104-66322009000100021
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